Crystallography Open Database

Information card for entry 4518770

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Coordinates	4518770.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H84 Ca2 N8
Calculated formula	C48 H84 Ca2 N8
Title of publication	Organocalcium Complex-Catalyzed Selective Redistribution of ArSiH3 or Ar(alkyl)SiH2 to Ar3SiH or Ar2(alkyl)SiH
Authors of publication	Li, Tao; McCabe, Karl N.; Maron, Laurent; Leng, Xuebing; Chen, Yaofeng
Journal of publication	ACS Catalysis
Year of publication	2021
Pages of publication	6348 - 6356
a	19.5031 ± 0.0005 Å
b	49.3831 ± 0.0015 Å
c	13.0859 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	12603.3 ± 0.6 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170.04 K
Number of distinct elements	4
Space group number	43
Hermann-Mauguin space group symbol	F d d 2
Hall space group symbol	F 2 -2d
Residual factor for all reflections	0.0633
Residual factor for significantly intense reflections	0.0478
Weighted residual factors for significantly intense reflections	0.1194
Weighted residual factors for all reflections included in the refinement	0.1313
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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