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Information card for entry 4518855
Preview
Coordinates | 4518855.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H15 F3 N0 O0 |
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Calculated formula | C22 H15 F3 |
Title of publication | Fluoroalkyl N-Triftosylhydrazones as Easily Decomposable Diazo Surrogates for Asymmetric [2 + 1] Cycloaddition: Synthesis of Chiral Fluoroalkyl Cyclopropenes and Cyclopropanes |
Authors of publication | Zhang, Xinyu; Tian, Chunqi; Wang, Zhanjing; Sivaguru, Paramasivam; Nolan, Steven P.; Bi, Xihe |
Journal of publication | ACS Catalysis |
Year of publication | 2021 |
Pages of publication | 8527 - 8537 |
a | 6.3512 ± 0.0005 Å |
b | 15.7186 ± 0.0013 Å |
c | 17.6114 ± 0.0017 Å |
α | 95.974 ± 0.007° |
β | 99.576 ± 0.007° |
γ | 94.985 ± 0.007° |
Cell volume | 1714.5 ± 0.3 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.1254 |
Residual factor for significantly intense reflections | 0.0544 |
Weighted residual factors for significantly intense reflections | 0.116 |
Weighted residual factors for all reflections included in the refinement | 0.1529 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.005 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4518855.html
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Users of the data should acknowledge the original authors of the
structural data.