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Information card for entry 4519251
Preview
Coordinates | 4519251.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H31 N O4 S |
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Calculated formula | C28 H31 N O4 S |
Title of publication | Cp*RhIII/Chiral Disulfonate/CuOAc Catalyst System for the Enantioselective Intramolecular Oxyamination of Alkenes |
Authors of publication | Hirose, Jumpei; Wakikawa, Takumi; Satake, Shun; Kojima, Masahiro; Hatano, Manabu; Ishihara, Kazuaki; Yoshino, Tatsuhiko; Matsunaga, Shigeki |
Journal of publication | ACS Catalysis |
Year of publication | 2021 |
Journal volume | 11 |
Journal issue | 24 |
Pages of publication | 15187 - 15193 |
a | 11.2477 ± 0.0007 Å |
b | 11.2911 ± 0.0007 Å |
c | 11.5245 ± 0.0007 Å |
α | 85.163 ± 0.004° |
β | 69.406 ± 0.003° |
γ | 65.577 ± 0.003° |
Cell volume | 1244.26 ± 0.14 Å3 |
Cell temperature | 233 ± 2 K |
Ambient diffraction temperature | 233 ± 2 K |
Number of distinct elements | 5 |
Space group number | 1 |
Hermann-Mauguin space group symbol | P 1 |
Hall space group symbol | P 1 |
Residual factor for all reflections | 0.0396 |
Residual factor for significantly intense reflections | 0.0377 |
Weighted residual factors for significantly intense reflections | 0.1048 |
Weighted residual factors for all reflections included in the refinement | 0.1062 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
Diffraction radiation wavelength | 1.5418 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4519251.html
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Users of the data should acknowledge the original authors of the
structural data.