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Information card for entry 4519383
Preview
Coordinates | 4519383.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C33 H50 N3 Ni O5 P |
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Calculated formula | C33 H50 N3 Ni O5 P |
Title of publication | Catalytic Synthesis of a Methylmalonate Salt from Ethylene and Carbon Dioxide through Photoinduced Activation and Photoredox-Catalyzed Reduction of Nickelalactones |
Authors of publication | Takahashi, Kohei; Sakurazawa, Yuji; Iwai, Asaki; Iwasawa, Nobuharu |
Journal of publication | ACS Catalysis |
Year of publication | 2022 |
Journal volume | 12 |
Journal issue | 7 |
Pages of publication | 3776 - 3781 |
a | 16.5365 ± 0.0009 Å |
b | 15.9821 ± 0.0006 Å |
c | 12.9995 ± 0.0006 Å |
α | 90° |
β | 97.271 ± 0.005° |
γ | 90° |
Cell volume | 3408 ± 0.3 Å3 |
Cell temperature | 123 K |
Ambient diffraction temperature | 123 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0849 |
Residual factor for significantly intense reflections | 0.0608 |
Weighted residual factors for significantly intense reflections | 0.1585 |
Weighted residual factors for all reflections included in the refinement | 0.1731 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.075 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4519383.html
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