Information card for entry 4519414

Structure parameters

• Formula: C28 H48 Cl6 N4 O8 Si2
• Calculated formula: C28 H48 Cl6 N4 O8 Si2
• Title of publication: Disilanes with Pentacoordinate Si Atoms by Carbon Dioxide Insertion into Aminodisilanes: Syntheses, Molecular Structures, and Dynamic Behavior.
• Authors of publication: Ryll, Christopher; Kraushaar, Konstantin; Wagler, Jörg; Brendler, Erica; Kroke, Edwin
• Journal of publication: ACS omega
• Year of publication: 2022
• Journal volume: 7
• Journal issue: 11
• Pages of publication: 9527 - 9536
• a: 9.3555 ± 0.0006 Å
• b: 19.1906 ± 0.0008 Å
• c: 10.8119 ± 0.0006 Å
• α: 90°
• β: 91.602 ± 0.005°
• γ: 90°
• Cell volume: 1940.38 ± 0.18 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0455
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0826
• Weighted residual factors for all reflections included in the refinement: 0.0893
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No