Information card for entry 5000311

Structure parameters

• Formula: C26 H55 Cl N3 O17 V5
• Calculated formula: C26 H55 Cl N3 O17 V5
• Title of publication: Stepwise assembly of a polyoxovanadate from mononuclear units in an organic solvent: carboxylate-stabilised fragments in the conversion of [VOCl4]2− to [V15O36]5−
• Authors of publication: Karet, Gail B.; Streib, William E.; Bollinger, John C.; Christou, George; Sun, Ziming; Hendrickson, David N.
• Journal of publication: Chemical Communications
• Journal issue: 22
• Pages of publication: 2249 - 2250
• a: 16.111 ± 0.002 Å
• b: 14.9003 ± 0.0019 Å
• c: 33.674 ± 0.005 Å
• α: 90°
• β: 91.39 ± 0.007°
• γ: 90°
• Cell volume: 8081 ± 3 ų
• Cell temperature: 101 K
• Ambient diffraction temperature: 101 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for all reflections included in the refinement: 0.0411
• Goodness-of-fit parameter for all reflections included in the refinement: 1.3432
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No