Information card for entry 5000354

Structure parameters

• Formula: C65 H72 Cl2 Mn4 N8 O22
• Calculated formula: C64.3333 H58 Cl2 Mn4 N8 O20.3333
• Title of publication: Tetranuclear Manganese Complexes with Dimer-of-Dimer and Ladder Structures from the Use of a Bis-Bipyridyl Ligand
• Authors of publication: E. Carolina Sañudo; Vincent A. Grillo; Michael J. Knapp; John C. Bollinger; John C. Huffman; David N. Hendrickson; George Christou
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 2441 - 2450
• a: 14.2186 ± 0.0006 Å
• b: 19.1159 ± 0.0008 Å
• c: 20.9052 ± 0.0009 Å
• α: 74.7132 ± 0.0012°
• β: 83.7498 ± 0.0012°
• γ: 68.737 ± 0.0012°
• Cell volume: 5107.3 ± 0.4 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 113 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for all reflections included in the refinement: 0.0511
• Goodness-of-fit parameter for all reflections included in the refinement: 1.6685
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No