Information card for entry 7000034

Structure parameters

• Formula: C28 H30 Cl F12 N8 P2 Rh
• Calculated formula: C28 H30 Cl F12 N8 P2 Rh
• Title of publication: A convenient synthetic route to half-sandwich rhodium(III) complexes of the tripodal ligand tris(3,5-dimethylpyrazolyl)methane.
• Authors of publication: Gonzalez, Veronica; Adams, Harry; Thomas, Jim A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 1
• Pages of publication: 110 - 115
• a: 8.8314 ± 0.0013 Å
• b: 11.1993 ± 0.0017 Å
• c: 33.99 ± 0.005 Å
• α: 90°
• β: 92.057 ± 0.003°
• γ: 90°
• Cell volume: 3359.6 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1084
• Residual factor for significantly intense reflections: 0.0688
• Weighted residual factors for significantly intense reflections: 0.1572
• Weighted residual factors for all reflections included in the refinement: 0.1753
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No