Information card for entry 7000105

Structure parameters

• Formula: C58 H52 Cl12 N2 P4 Pd2
• Calculated formula: C55 H46 Cl6 N2 P4 Pd2
• Title of publication: Oligodentate P,N ligands: N,N,N',N'-tetrakis(diphenylphosphanyl)-1,3-diaminobenzene complexes of rhodium, nickel and palladium.
• Authors of publication: Majoumo-Mbe, Félicité; Lönnecke, Peter; Novikova, Elena V.; Belov, Gennadiy P.; Hey-Hawkins, Evamarie
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 20
• Pages of publication: 3326 - 3330
• a: 17.592 ± 0.002 Å
• b: 22.333 ± 0.003 Å
• c: 16.92 ± 0.002 Å
• α: 90°
• β: 96.097 ± 0.002°
• γ: 90°
• Cell volume: 6610 ± 1.4 ų
• Cell temperature: 208 ± 2 K
• Ambient diffraction temperature: 208 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0697
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.1226
• Weighted residual factors for all reflections included in the refinement: 0.1342
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No