Information card for entry 7000152

Structure parameters

• Formula: C25 H35 F4 N Ni P2
• Calculated formula: C24.998 H35 F4 N0.998 Ni P2
• Title of publication: C-F Bond activation at Ni(0) and simple reactions of square planar Ni(II) fluoride complexes.
• Authors of publication: Burling, Suzanne; Elliott, Paul I. P.; Jasim, Naser A.; Lindup, Richard J.; McKenna, Jennifer; Perutz, Robin N.; Archibald, Stephen J.; Whitwood, Adrian C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 22
• Pages of publication: 3686 - 3695
• a: 30.943 ± 0.004 Å
• b: 30.943 ± 0.004 Å
• c: 11.522 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11032 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.3019
• Residual factor for significantly intense reflections: 0.0617
• Weighted residual factors for significantly intense reflections: 0.1354
• Weighted residual factors for all reflections included in the refinement: 0.2219
• Goodness-of-fit parameter for all reflections included in the refinement: 0.955
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No