Information card for entry 7000164

Structure parameters

• Formula: C59 H76 Ga4 O12 Rh6
• Calculated formula: C59 H76 Ga4 O12 Rh6
• Title of publication: Novel rhodium and ruthenium carbonyl cluster complexes with face- and edge-bridging GaCp* ligands. Synthesis and structural characterization of the Rh6(CO)12(mu3-GaCp*)4 and Ru6(eta6-C)(mu2-CO)(CO)13(mu3-GaCp*)2(mu2-GaCp*) clusters.
• Authors of publication: Grachova, Elena V.; Jutzi, Peter; Neumann, Beate; Stammler, Hans-Georg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 22
• Pages of publication: 3614 - 3616
• a: 15.866 ± 0.0014 Å
• b: 15.866 ± 0.002 Å
• c: 12.6 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3171.8 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 82
• Hermann-Mauguin space group symbol: I -4
• Hall space group symbol: I -4
• Residual factor for all reflections: 0.0284
• Residual factor for significantly intense reflections: 0.0212
• Weighted residual factors for significantly intense reflections: 0.0384
• Weighted residual factors for all reflections included in the refinement: 0.0403
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No