Information card for entry 7000194

Structure parameters

• Formula: C96 H246 N24 Ni6 O90 V32
• Calculated formula: C96 H216 N24 Ni6 O90 V32
• Title of publication: Vanadium polyoxoanion-bridged macrocyclic metal complexes: from one-dimensional to three-dimensional structures
• Authors of publication: Ou, Guang-Chuan; Jiang, Long; Feng, Xiao-Long; Lu, Tong-Bu
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 1
• Pages of publication: 71 - 76
• a: 13.482 ± 0.003 Å
• b: 25.8 ± 0.003 Å
• c: 26.521 ± 0.003 Å
• α: 90°
• β: 92.2 ± 0.003°
• γ: 90°
• Cell volume: 9218 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0675
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.126
• Weighted residual factors for all reflections included in the refinement: 0.1339
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No