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Information card for entry 7000238
Preview
Coordinates | 7000238.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C56 H60 P6 Pt2 |
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Calculated formula | C56 H60 P6 Pt2 |
SMILES | [Pt]1(P2[Pt](P12)([P](CC)(c1ccccc1)c1ccccc1)[P](CC)(c1ccccc1)c1ccccc1)([P](CC)(c1ccccc1)c1ccccc1)[P](CC)(c1ccccc1)c1ccccc1 |
Title of publication | Reactions of R2P‒P(SiMe3)Li with [(R′3P)2PtCl2]. A general and efficient entry to phosphanylphosphinidene complexes of platinum. Syntheses and structures of [(η2-PPiPr2)Pt(p-Tol3P)2], [(η2-PPtBu2)Pt(p-Tol3P)2], [{η2-PP(NiPr2)2}Pt(p-Tol3P)2] and [{(Et2PhP)2Pt}2P2] |
Authors of publication | Domańska-Babul, Wioleta; Chojnacki, Jaroslaw; Matern, Eberhard; Pikies, Jerzy |
Journal of publication | Dalton Transactions |
Year of publication | 2009 |
Journal issue | 1 |
Pages of publication | 146 - 151 |
a | 19.5441 ± 0.0016 Å |
b | 9.6862 ± 0.001 Å |
c | 29.7907 ± 0.0017 Å |
α | 90° |
β | 107.751 ± 0.009° |
γ | 90° |
Cell volume | 5371.1 ± 0.8 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1777 |
Residual factor for significantly intense reflections | 0.1227 |
Weighted residual factors for significantly intense reflections | 0.2875 |
Weighted residual factors for all reflections included in the refinement | 0.3115 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.14 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7000238.html
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