Crystallography Open Database

Information card for entry 7000371

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Coordinates	7000371.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H32 B F24 N4 Rh
Calculated formula	C47 H32 B F24 N4 Rh
Title of publication	Weakly coordinating counter-ions for highly efficient catalysis of intramolecular hydroamination
Authors of publication	Dabb, Serin L.; Ho, Joanne H. H.; Hodgson, Richard; Messerle, Barbara A.; Wagler, Jörg
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	4
Pages of publication	634
a	13.0057 ± 0.0002 Å
b	13.6112 ± 0.0002 Å
c	15.8258 ± 0.0003 Å
α	68.912 ± 0.001°
β	69.271 ± 0.001°
γ	68.368 ± 0.001°
Cell volume	2349.38 ± 0.07 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0589
Residual factor for significantly intense reflections	0.0478
Weighted residual factors for significantly intense reflections	0.1267
Weighted residual factors for all reflections included in the refinement	0.1323
Goodness-of-fit parameter for all reflections included in the refinement	1.068
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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