Information card for entry 7000380

Structure parameters

• Formula: C59.88 H66.75 Al Cl3.75 F36 Ge O10
• Calculated formula: C59.88 H66.76 Al Cl3.76 F36 Ge O10
• Title of publication: [(OtBu)2C6H3]3Ge+ a free germyl cation with aryl ligands
• Authors of publication: Schenk, Christian; Drost, Christian; Schnepf, Andreas
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 5
• Pages of publication: 773 - 776
• a: 18.101 ± 0.0009 Å
• b: 24.3749 ± 0.0008 Å
• c: 18.2722 ± 0.0008 Å
• α: 90°
• β: 106.088 ± 0.004°
• γ: 90°
• Cell volume: 7746.2 ± 0.6 ų
• Cell temperature: 99 ± 2 K
• Ambient diffraction temperature: 99 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0569
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.1068
• Weighted residual factors for all reflections included in the refinement: 0.1138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No