Information card for entry 7000392

Structure parameters

• Formula: C39.5 H39 Cl3 Co2 I4 N2 O2 P2
• Calculated formula: C39.5 H39 Cl3 Co2 I4 N2 O2 P2
• Title of publication: Synthesis and characterization of Co and Ni complexes stabilized by keto- and acetamide-derived P,O-type phosphine ligands
• Authors of publication: Agostinho, Magno; Rosa, Vitor; Avilés, Teresa; Welter, Richard; Braunstein, Pierre
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 5
• Pages of publication: 814 - 822
• a: 8.052 ± 0.0003 Å
• b: 15.407 ± 0.0005 Å
• c: 19.874 ± 0.0007 Å
• α: 89.393 ± 0.002°
• β: 82.027 ± 0.002°
• γ: 76.374 ± 0.0014°
• Cell volume: 2372.33 ± 0.15 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.114
• Residual factor for significantly intense reflections: 0.0593
• Weighted residual factors for significantly intense reflections: 0.1627
• Weighted residual factors for all reflections included in the refinement: 0.1971
• Goodness-of-fit parameter for all reflections included in the refinement: 0.912
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No