Information card for entry 7000399

Structure parameters

• Common name: aqua(N,N'-bis(o-fluorophenyl)diaza-18-crown- 6)lead(ii)diperchlorate
• Chemical name: aqua{N,N'-bis(o-fluorophenyl)diaza-18-crown-6}lead(II)diperchlorate
• Formula: C24 H34 Cl2 F2 N2 O13 Pb
• Calculated formula: C24 H34 Cl2 F2 N2 O13 Pb
• Title of publication: Lariat ethers with fluoroaryl side-arms: a study of CF⋯metal cation interaction in the complexes of N-(o-fluoroaryl)azacrown ethers
• Authors of publication: Sazonov, Petr K.; Minacheva, Lidiya Kh.; Churakov, Andrei V.; Sergienko, Vladimir S.; Artamkina, Galina A.; Oprunenko, Yuri F.; Beletskaya, Irina P.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 5
• Pages of publication: 843 - 850
• a: 19.423 ± 0.005 Å
• b: 12.719 ± 0.003 Å
• c: 13.109 ± 0.003 Å
• α: 90°
• β: 94.711 ± 0.003°
• γ: 90°
• Cell volume: 3227.5 ± 1.3 ų
• Cell temperature: 303 ± 2 K
• Ambient diffraction temperature: 303 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0893
• Residual factor for significantly intense reflections: 0.0679
• Weighted residual factors for significantly intense reflections: 0.1773
• Weighted residual factors for all reflections included in the refinement: 0.1967
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No