Information card for entry 7000407

Structure parameters

• Formula: C37 H30 Cl6 N4 Pd
• Calculated formula: C37 H30 Cl6 N4 Pd
• Title of publication: Direct synthesis of a new class of N,N,N ligands based on 1,2-dihydro-1,10-phenanthroline backbone and their coordination to Pd complexes
• Authors of publication: Rangheard, Claudine; Proriol, David; Olivier-Bourbigou, Hélène; Braunstein, Pierre
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 5
• Pages of publication: 770 - 772
• a: 10.9448 ± 0.0004 Å
• b: 12.9038 ± 0.0006 Å
• c: 13.8457 ± 0.0006 Å
• α: 80.351 ± 0.002°
• β: 86.891 ± 0.002°
• γ: 67.035 ± 0.002°
• Cell volume: 1774.84 ± 0.13 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1008
• Residual factor for significantly intense reflections: 0.0727
• Weighted residual factors for significantly intense reflections: 0.146
• Weighted residual factors for all reflections included in the refinement: 0.1589
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No