Metal and ligand substitution of the aluminium tris-pyridyl ligands [RAl(2-py′)3]− (R = Et, nBu, sBu, tBu; 2-py′ = 2-pyridyl, 3-methyl-2-pyridyl, 5-methyl-2-pyridyl, 6-methyl-2-pyridyl)
Authors of publication
Bullock, Thomas H.; Chan, Wesley T. K.; Eisler, Dana J.; Streib, Manuel; Wright, Dominic S.
Journal of publication
Dalton Transactions
Year of publication
2009
Journal issue
6
Pages of publication
1046 - 1054
a
10.6809 ± 0.0002 Å
b
20.5331 ± 0.0004 Å
c
15.2723 ± 0.0003 Å
α
90°
β
93.2816 ± 0.0009°
γ
90°
Cell volume
3343.91 ± 0.11 Å3
Cell temperature
180 ± 2 K
Ambient diffraction temperature
180 ± 2 K
Number of distinct elements
8
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0934
Residual factor for significantly intense reflections
0.0628
Weighted residual factors for significantly intense reflections
0.1486
Weighted residual factors for all reflections included in the refinement
0.17
Goodness-of-fit parameter for all reflections included in the refinement
