Information card for entry 7000544

Structure parameters

• Formula: C36 H54 N4 O2 Re6 S8
• Calculated formula: C36 H16 N4 O2 Re6 S8
• Title of publication: Selective functionalisation of Re6 cluster anionic units: from hexa-hydroxo [Re6Q8(OH)6]4− (Q = S, Se) to neutral trans-[Re6Q8L4L′2] hybrid building blocks
• Authors of publication: Dorson, Frédérick; Molard, Yann; Cordier, Stéphane; Fabre, Bruno; Efremova, Olga; Rondeau, David; Mironov, Yuri; Cîrcu, Viorel; Naumov, Nikolay; Perrin, Christiane
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 8
• Pages of publication: 1297
• a: 18.3921 ± 0.0005 Å
• b: 17.994 ± 0.0006 Å
• c: 9.1061 ± 0.0003 Å
• α: 90°
• β: 105.99 ± 0.001°
• γ: 90°
• Cell volume: 2897.04 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for all reflections included in the refinement: 0.1035
• Goodness-of-fit parameter for all reflections included in the refinement: 1.154
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No