Information card for entry 7000670

Structure parameters

• Common name: (eta$3!-allyl)-tris-(triphenyl-stibine)-nickel(ii) tetrakis- (3,5-bis-trifluoromethyl-phenyl)-borate dichloromethane solvate
• Chemical name: (η^3^-allyl)-tris-(triphenyl-stibine)-nickel(II) tetrakis-(3,5-bis-trifluoromethyl-phenyl)-borate dichloromethane solvate
• Formula: C89.86 H63.71 B Cl1.71 F24 Ni Sb3
• Calculated formula: C89.857 H63.714 B Cl1.714 F24 Ni Sb3
• Title of publication: Oligomerization of styrenes mediated by cationic allyl nickel complexes containing triphenylstibine or triphenylarsine
• Authors of publication: Jiménez-Tenorio, Manuel; Carmen Puerta, M.; Salcedo, Isabel; Valerga, Pedro; de los Ríos, Isaac; Mereiter, Kurt
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 10
• Pages of publication: 1842 - 1852
• a: 13.2682 ± 0.0006 Å
• b: 17.6246 ± 0.0007 Å
• c: 19.2441 ± 0.0008 Å
• α: 68.634 ± 0.001°
• β: 84.927 ± 0.001°
• γ: 87.387 ± 0.001°
• Cell volume: 4174 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0347
• Residual factor for significantly intense reflections: 0.0304
• Weighted residual factors for significantly intense reflections: 0.0737
• Weighted residual factors for all reflections included in the refinement: 0.0759
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No