Information card for entry 7000837

Structure parameters

• Formula: C31 H55 N3 O Si4 Yb
• Calculated formula: C31 H55 N3 O Si4 Yb
• Title of publication: Heteroleptic ytterbium(ii) complexes supported by a bulky β-diketiminato ligand
• Authors of publication: Hitchcock, Peter B.; Khvostov, Alexei V.; Lappert, Michael F.; Protchenko, Andrey V.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 13
• Pages of publication: 2383 - 2391
• a: 9.8514 ± 0.0002 Å
• b: 21.2659 ± 0.0004 Å
• c: 19.0709 ± 0.0004 Å
• α: 90°
• β: 101.922 ± 0.001°
• γ: 90°
• Cell volume: 3909.15 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0422
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.0602
• Weighted residual factors for all reflections included in the refinement: 0.0646
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No