Information card for entry 7001017

Structure parameters

• Formula: C20 H33 Cl2 Ir2 N
• Calculated formula: C20 H33 Cl2 Ir2 N
• SMILES: [c]12([c]3([c]4([c]5([c]1(C)[Ir]162345([H][Ir]23456([NH2]1)([c]1([c]2([c]3([c]4([c]51C)C)C)C)C)Cl)Cl)C)C)C)C
• Title of publication: Synthesis of parent amido (NH2)-bridged dinuclear complexes of ruthenium and iridium by stepwise transfer hydrogenation of μ-azido complexes
• Authors of publication: Kimura, Takashi; Arita, Hiroko; Ishiwata, Koji; Kuwata, Shigeki; Ikariya, Takao
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 16
• Pages of publication: 2912 - 2914
• a: 19.25 ± 0.009 Å
• b: 13.076 ± 0.006 Å
• c: 9.06 ± 0.004 Å
• α: 90°
• β: 92.449 ± 0.008°
• γ: 90°
• Cell volume: 2278.4 ± 1.8 ų
• Cell temperature: 293.1 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for all reflections included in the refinement: 0.098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No