Sulfato-bridged ECE-pincer palladium(ii) complexes: structures in the solid-state and in solution, and catalytic properties
Authors of publication
Kruithof, Cornelis A.; Berger, Alexsandro; Dijkstra, Harmen P.; Soulimani, Fouad; Visser, Tom; Lutz, Martin; Spek, Anthony L.; Gebbink, Robertus J. M. Klein; van Koten, Gerard
Journal of publication
Dalton Transactions
Year of publication
2009
Journal issue
17
Pages of publication
3306 - 3314
a
15.5104 ± 0.0006 Å
b
14.0482 ± 0.0006 Å
c
17.2217 ± 0.0013 Å
α
90°
β
101.7 ± 0.005°
γ
90°
Cell volume
3674.5 ± 0.4 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0242
Residual factor for significantly intense reflections
0.0191
Weighted residual factors for significantly intense reflections
0.0447
Weighted residual factors for all reflections included in the refinement
0.0464
Goodness-of-fit parameter for all reflections included in the refinement
