Information card for entry 7001228

Structure parameters

• Formula: C42 H45 F3 I2 P3 Rh
• Calculated formula: C42 H45 F3 I2 P3 Rh
• Title of publication: Synthesis of rhodium(i) and rhodium(iii) perfluoroalkyl complexes from [Rh(μ-OH)(COD)]2
• Authors of publication: Vicente, José; Gil-Rubio, Juan; Guerrero-Leal, Juan; Bautista, Delia
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 19
• Pages of publication: 3854 - 3866
• a: 10.2462 ± 0.0007 Å
• b: 17.9511 ± 0.0012 Å
• c: 22.2871 ± 0.0015 Å
• α: 90°
• β: 99.995 ± 0.002°
• γ: 90°
• Cell volume: 4037.1 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0335
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for significantly intense reflections: 0.0742
• Weighted residual factors for all reflections included in the refinement: 0.075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.153
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No