Information card for entry 7001258

Structure parameters

• Formula: C76.6 H69.2 B2 Cl5.2 F8 Fe2 N2 P4 Pd2 S4
• Calculated formula: C76.6 H69.2 B2 Cl5.2 F8 Fe2 N2 P4 Pd2 S4
• Title of publication: Multimetallic arrays: Symmetrical bi-, tri- and tetrametallic complexes based on the group 10 metals and the functionalisation of gold nanoparticles with nickel-phosphine surface units
• Authors of publication: Knight, Edward R.; Leung, Nina H.; Lin, Yvonne H.; Cowley, Andrew R.; Watkin, David J.; Thompson, Amber L.; Hogarth, Graeme; Wilton-Ely, James D. E. T.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 19
• Pages of publication: 3688 - 3697
• a: 10.5409 ± 0.0002 Å
• b: 18.8334 ± 0.0003 Å
• c: 21.279 ± 0.0004 Å
• α: 90°
• β: 97.2552 ± 0.0008°
• γ: 90°
• Cell volume: 4190.51 ± 0.13 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 10
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0948
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for all reflections: 0.0959
• Weighted residual factors for significantly intense reflections: 0.0598
• Weighted residual factors for all reflections included in the refinement: 0.0558
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0797
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No