Information card for entry 7001481

Structure parameters

• Formula: C52 H62 Cl N3 Nb O4.5
• Calculated formula: C52 H62 Cl N3 Nb O4.5
• Title of publication: Mono-anionic acetophenone imine ligands: synthesis, ortho-lithiation and first examples of group (v) metal complexes
• Authors of publication: Neshat, Abdollah; Seambos, Cheryl L.; Beck, John F.; Schmidt, Joseph A. R.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 25
• Pages of publication: 4987 - 5000
• a: 9.557 ± 0.001 Å
• b: 12.424 ± 0.002 Å
• c: 21.471 ± 0.003 Å
• α: 106.767 ± 0.003°
• β: 91.047 ± 0.003°
• γ: 101.57 ± 0.003°
• Cell volume: 2383.5 ± 0.6 ų
• Cell temperature: 175 ± 2 K
• Ambient diffraction temperature: 175 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.12
• Residual factor for significantly intense reflections: 0.0814
• Weighted residual factors for significantly intense reflections: 0.205
• Weighted residual factors for all reflections included in the refinement: 0.234
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No