Information card for entry 7001496

Structure parameters

• Formula: C48 H92.5 Ag3 N9 O22.25
• Calculated formula: C48 H90 Ag3 N9 O22.25
• Title of publication: Polymeric di- and discrete trinuclear silver(I) assemblies incorporating γ-carbon bonded, neutral acetylacetone-imine motifs assembled from racemic and diastereopure N,N′-bis(acetylacetone)cyclohexanediimine units
• Authors of publication: Zhu, Bi-Xue; Zhang, Qi-Long; Zhang, Yun-Qian; Tao, Zhu; Clegg, Jack K.; Reimers, Jeffrey R.; Lindoy, Leonard F.; Wei, Gang
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 25
• Pages of publication: 4896 - 4900
• a: 15.9158 ± 0.0013 Å
• b: 15.9158 ± 0.0013 Å
• c: 43.304 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 9499.8 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 155
• Hermann-Mauguin space group symbol: R 3 2 :H
• Hall space group symbol: R 3 2"
• Residual factor for all reflections: 0.0351
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.0953
• Weighted residual factors for all reflections included in the refinement: 0.0965
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No