Information card for entry 7001564

Structure parameters

• Formula: C62 H72 O6 Sb2
• Calculated formula: C62 H72 O6 Sb2
• Title of publication: Synthesis, X-ray structures and reactivity of calix[5]arene bismuth(iii) and antimony(iii) complexes
• Authors of publication: Mendoza-Espinosa, Daniel; Hanna, Tracy A.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 26
• Pages of publication: 5211 - 5225
• a: 14.411 ± 0.004 Å
• b: 16.183 ± 0.004 Å
• c: 16.211 ± 0.004 Å
• α: 94.706 ± 0.005°
• β: 109.515 ± 0.005°
• γ: 105.495 ± 0.005°
• Cell volume: 3372.3 ± 1.5 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1003
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for significantly intense reflections: 0.1993
• Weighted residual factors for all reflections included in the refinement: 0.2224
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No