Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7001680
Preview
Coordinates | 7001680.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C14 H67 Ge N7 O67 P2 W17 |
---|---|
Calculated formula | C8 N4 O66 P2 W18 |
SMILES | C[NH2+]C.C[NH2+]C.C[NH2+]C.C[NH2+]C.O=[W]1234O[W]567(=O)O[W]89(=O)(O1)O[W]1%10%11(O[W]%12%13(O6)(O[W]6%14(O5)(O[W]5%15(O2)(O[W]2%16(O3)(O[W](O8)(O1)(=O)([O]2=P([O]479)([O]65)[O]%10%12)O[W]123(O[W]45(O%11)(O[W]67(O%13)(O[W]89(O%14)(O[W]%10%11(O%15)(O[W]%12(O%16)(O1)(=O)[O]2=P([O]8%10)([O]46)[O]12[W]4(O%11)(O%12)(=O)O[W]1(O9)(O7)(=O)O[W]2(O5)(O3)(=O)O4)=O)=O)=O)=O)=O)=O)=O)=O)=O)=O.O.O.O.O |
Title of publication | Cyclic oligomer of oxide clusters through a siloxane bond. Synthesis and structure of reaction products of α2-mono-lacunary Dawson polyoxometalate with tetrachlorosilane and tetraethoxysilane |
Authors of publication | Kurashina, Takayuki; Aoki, Shotaro; Hirasawa, Ryota; Hasegawa, Takeshi; Kasahara, Yuhki; Yoshida, Shoko; Yoza, Kenji; Nomiya, Kenji |
Journal of publication | Dalton Transactions |
Year of publication | 2009 |
Journal issue | 28 |
Pages of publication | 5542 - 5550 |
a | 12.9435 ± 0.0012 Å |
b | 13.2455 ± 0.0013 Å |
c | 23.588 ± 0.002 Å |
α | 81.049 ± 0.001° |
β | 85.485 ± 0.001° |
γ | 68.512 ± 0.001° |
Cell volume | 3716.1 ± 0.6 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1047 |
Residual factor for significantly intense reflections | 0.0651 |
Weighted residual factors for significantly intense reflections | 0.1728 |
Weighted residual factors for all reflections included in the refinement | 0.1986 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.103 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7001680.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.