Information card for entry 7001684

Structure parameters

• Formula: C67 H92 N4 Ni Si2
• Calculated formula: C67 H92 N4 Ni Si2
• Title of publication: N-Aryl substituted heterocyclic silylenes
• Authors of publication: Kong, Lingbing; Zhang, Jianying; Song, Haibin; Cui, Chunming
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 28
• Pages of publication: 5444 - 5446
• a: 13.558 ± 0.003 Å
• b: 18.331 ± 0.004 Å
• c: 24.29 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6037 ± 2 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.1007
• Residual factor for significantly intense reflections: 0.0651
• Weighted residual factors for significantly intense reflections: 0.1403
• Weighted residual factors for all reflections included in the refinement: 0.1557
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No