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Information card for entry 7001721
Preview
Coordinates | 7001721.cif |
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Original paper (by DOI) | HTML |
Formula | C30 H42 N12 Si2 |
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Calculated formula | C30 H42 N12 Si2 |
Title of publication | Syntheses, structures, and reactivity of poly(pyrazolyl)silanes, -disilanes, and the ambidentate κ1Si/κ3N-coordinating tris(3,5-dimethylpyrazolyl)silanide ligand [Si(3,5-Me2pz)3]− (MeTpsd) |
Authors of publication | Armbruster, Felix; Fernández, Ignacio; Breher, Frank |
Journal of publication | Dalton Transactions |
Year of publication | 2009 |
Journal issue | 29 |
Pages of publication | 5612 - 5626 |
a | 7.972 ± 0.0016 Å |
b | 13.566 ± 0.003 Å |
c | 15.596 ± 0.003 Å |
α | 76.99 ± 0.03° |
β | 83.98 ± 0.03° |
γ | 83.97 ± 0.03° |
Cell volume | 1628.5 ± 0.6 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1133 |
Residual factor for significantly intense reflections | 0.0624 |
Weighted residual factors for significantly intense reflections | 0.1456 |
Weighted residual factors for all reflections included in the refinement | 0.1736 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.935 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7001721.html
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