Syntheses, structures, and reactivity of poly(pyrazolyl)silanes, -disilanes, and the ambidentate κ1Si/κ3N-coordinating tris(3,5-dimethylpyrazolyl)silanide ligand [Si(3,5-Me2pz)3]− (MeTpsd)
Authors of publication
Armbruster, Felix; Fernández, Ignacio; Breher, Frank
Journal of publication
Dalton Transactions
Year of publication
2009
Journal issue
29
Pages of publication
5612 - 5626
a
16.497 ± 0.002 Å
b
16.497 ± 0.002 Å
c
16.497 ± 0.002 Å
α
90°
β
90°
γ
90°
Cell volume
4489.7 ± 0.9 Å3
Cell temperature
200 ± 2 K
Ambient diffraction temperature
200 ± 2 K
Number of distinct elements
4
Space group number
197
Hermann-Mauguin space group symbol
I 2 3
Hall space group symbol
I 2 2 3
Residual factor for all reflections
0.0387
Residual factor for significantly intense reflections
0.0383
Weighted residual factors for significantly intense reflections
0.0923
Weighted residual factors for all reflections included in the refinement
0.093
Goodness-of-fit parameter for all reflections included in the refinement
