Information card for entry 7001815

Structure parameters

• Formula: C6 H40 As K Na6 O51 Ru W9
• Calculated formula: C6 H6 As K Na6 O53 Ru W9
• Title of publication: Synthesis and crystal structure of pseudo-sandwich-type heteropolytungstates functionalized by organometallic ruthenium(ii)
• Authors of publication: Bi, Li-Hua; Hou, Guang-Feng; Li, Bao; Wu, Li-Xin; Kortz, Ulrich
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 32
• Pages of publication: 6345 - 6353
• a: 15.1433 ± 0.0012 Å
• b: 16.8981 ± 0.0013 Å
• c: 19.8968 ± 0.0016 Å
• α: 90°
• β: 90.861 ± 0.001°
• γ: 90°
• Cell volume: 5090.9 ± 0.7 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0479
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0784
• Weighted residual factors for all reflections included in the refinement: 0.0809
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No