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Information card for entry 7001836
Preview
Coordinates | 7001836.cif |
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Original paper (by DOI) | HTML |
Formula | C25 H38 N5 P Pd |
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Calculated formula | C25 H38 N5 P Pd |
SMILES | [Pd]1(C(=Nc2c(cccc2C(C)C)C(C)C)c2c(C[N]1(C)C)cccc2)([P](C)(C)C)N=N#N |
Title of publication | Cyclopalladated azido complexes containing C,N-donor (HCσim N = 2-(2′-thienyl)pyridine, azobenzene, 3,3′-dimethyl azobenzene, N,N′-dimethylbenzylamine, 2-phenylpyridine) ligands: reactivity towards organic unsaturated compounds and catalytic properties |
Authors of publication | Lee, Kyung-Eun; Jeon, Hyeong-Tak; Han, Sam-Yong; Ham, Jungyeob; Kim, Yong-Joo; Lee, Soon W. |
Journal of publication | Dalton Transactions |
Year of publication | 2009 |
Journal issue | 33 |
Pages of publication | 6578 - 6592 |
a | 12.0749 ± 0.0017 Å |
b | 10.95 ± 0.003 Å |
c | 20.463 ± 0.005 Å |
α | 90° |
β | 100.344 ± 0.012° |
γ | 90° |
Cell volume | 2661.6 ± 1.1 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0631 |
Residual factor for significantly intense reflections | 0.0396 |
Weighted residual factors for significantly intense reflections | 0.0853 |
Weighted residual factors for all reflections included in the refinement | 0.0957 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.018 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7001836.html
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