Information card for entry 7001938

Structure parameters

• Formula: C25 H31 Cl4 N4 V
• Calculated formula: C25 H31 Cl4 N4 V
• Title of publication: Synthesis and structure of early transition metal NHC complexes
• Authors of publication: Lorber, Christian; Vendier, Laure
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 35
• Pages of publication: 6972
• a: 8.5259 ± 0.0015 Å
• b: 13.09 ± 0.003 Å
• c: 14.3003 ± 0.0019 Å
• α: 63.734 ± 0.016°
• β: 79.869 ± 0.013°
• γ: 81.14 ± 0.015°
• Cell volume: 1403.6 ± 0.5 ų
• Cell temperature: 180 K
• Ambient diffraction temperature: 180 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1308
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.0713
• Weighted residual factors for all reflections included in the refinement: 0.0893
• Goodness-of-fit parameter for all reflections included in the refinement: 0.824
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No