Information card for entry 7001956

Structure parameters

• Formula: C227 H198 Au4 Cl6 F24 Mn4 N8 O16 P16
• Calculated formula: C227 H190 Au4 Cl6 F24 Mn4 N8 O16 P16
• Title of publication: NHC‒manganese(i) complexes as carbene transfer agents
• Authors of publication: Ruiz, Javier; Berros, Ángela; Perandones, Bernabé F.; Vivanco, Marilín
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 35
• Pages of publication: 6999
• a: 19.1731 ± 0.0008 Å
• b: 34.8321 ± 0.0017 Å
• c: 17.7003 ± 0.0009 Å
• α: 90°
• β: 106.796 ± 0.002°
• γ: 90°
• Cell volume: 11316.7 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.094
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1486
• Weighted residual factors for all reflections included in the refinement: 0.1591
• Goodness-of-fit parameter for all reflections included in the refinement: 1.579
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No