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Information card for entry 7001967
Preview
Coordinates | 7001967.cif |
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Original paper (by DOI) | HTML |
Formula | C59 H65 Fe N5 Si2 |
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Calculated formula | C59 H65 Fe N5 Si2 |
SMILES | c1(c(cccc1C(C)C)C(C)C)N1C2N(C=C1)c1[n]3[Fe]4=2([H][H]4)(=C2N(c4c(cccc4C(C)C)C(C)C)C=CN2c3ccc1)([SiH](c1ccccc1)c1ccccc1)[SiH](c1ccccc1)c1ccccc1 |
Title of publication | Reactions of ‘pincer’ pyridine dicarbene complexes of Fe(0) with silanes |
Authors of publication | Pugh, David; Wells, Neil J.; Evans, David J.; Danopoulos, Andreas A. |
Journal of publication | Dalton Transactions |
Year of publication | 2009 |
Journal issue | 35 |
Pages of publication | 7189 |
a | 23.466 ± 0.005 Å |
b | 10.382 ± 0.002 Å |
c | 22.594 ± 0.004 Å |
α | 90° |
β | 111.47 ± 0.03° |
γ | 90° |
Cell volume | 5122 ± 2 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0572 |
Residual factor for significantly intense reflections | 0.0407 |
Weighted residual factors for significantly intense reflections | 0.0985 |
Weighted residual factors for all reflections included in the refinement | 0.1065 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.03 |
Diffraction radiation wavelength | 0.8462 Å |
Diffraction radiation type | synchrotron |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7001967.html
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