Information card for entry 7002179

Structure parameters

• Formula: C48 H108 N3 O19 W6
• Calculated formula: C48 H108 N3 O19 W6
• Title of publication: A new synthetic route to Lindqvist type clusters [(n-Bu4N)x][M′M5O19] [when x = 2, M′ = M = Mo or W; x = 3, M′ = Mo, M = W] from metal carbonyl precursors [(CO)5ML] [M = Mo, W; L= CO, C(OMe)(Me)]
• Authors of publication: Thakur, Arunabha; Chakraborty, Amarnath; Ramkumar, V.; Ghosh, Sundargopal
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 36
• Pages of publication: 7552 - 7558
• a: 29.3874 ± 0.0018 Å
• b: 18.5641 ± 0.0018 Å
• c: 27.336 ± 0.002 Å
• α: 90°
• β: 113.085 ± 0.005°
• γ: 90°
• Cell volume: 13719 ± 1.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0509
• Residual factor for significantly intense reflections: 0.0316
• Weighted residual factors for significantly intense reflections: 0.0784
• Weighted residual factors for all reflections included in the refinement: 0.0906
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No