Information card for entry 7002210

Structure parameters

• Formula: C46 H46 B14 Co4 Fe2 N2 O20
• Calculated formula: C46 H46 B14 Co4 Fe2 N2 O20
• Title of publication: Ten-vertex {closo-2,1,10-FeC2B7} clusters with intramolecular imidate linkages: anchors for supramolecular construction
• Authors of publication: Franken, Andreas; McGrath, Thomas D.; Stone, F. Gordon A.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 36
• Pages of publication: 7353 - 7355
• a: 9.5889 ± 0.0014 Å
• b: 27.343 ± 0.004 Å
• c: 23.776 ± 0.004 Å
• α: 90°
• β: 100.028 ± 0.002°
• γ: 90°
• Cell volume: 6138.6 ± 1.6 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0907
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.0937
• Weighted residual factors for all reflections included in the refinement: 0.1114
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No