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Information card for entry 7002228
Preview
Coordinates | 7002228.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C56.5 H61 Cl4 N2 O3 P Pd |
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Calculated formula | C56.5 H61 Cl4 N2 O3 P Pd |
Title of publication | Chiral triaryl phosphite-based palladacycles and platinacycles: synthesis and application to asymmetric Lewis acid catalysis |
Authors of publication | Bedford, Robin B.; Dumycz, Helena; Haddow, Mairi F.; Pilarski, Lukasz T.; Orpen, A. Guy; Pringle, Paul G.; Wingad, Richard L. |
Journal of publication | Dalton Transactions |
Year of publication | 2009 |
Journal issue | 37 |
Pages of publication | 7796 - 7804 |
a | 14.495 ± 0.003 Å |
b | 16.679 ± 0.003 Å |
c | 21.684 ± 0.004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5242.4 ± 1.7 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0344 |
Residual factor for significantly intense reflections | 0.0329 |
Weighted residual factors for significantly intense reflections | 0.0879 |
Weighted residual factors for all reflections included in the refinement | 0.0891 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.074 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7002228.html
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