Information card for entry 7002262

Structure parameters

• Formula: C35.5 H54.5 Cl7.5 Co2 N4 O3
• Calculated formula: C35.5 H54.5 Cl7.5 Co2 N4 O3
• Title of publication: Structural and magnetic variability of cobalt(II) complexes with bridging pyrazolate ligands bearing appended imine groups
• Authors of publication: Sachse, Anna; Demeshko, Serhiy; Meyer, Franc
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 37
• Pages of publication: 7756 - 7764
• a: 16.3211 ± 0.0011 Å
• b: 17.7522 ± 0.0011 Å
• c: 31.585 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9151.3 ± 1.2 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 45
• Hermann-Mauguin space group symbol: I b a 2
• Hall space group symbol: I 2 -2c
• Residual factor for all reflections: 0.0314
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0754
• Weighted residual factors for all reflections included in the refinement: 0.0761
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No