Information card for entry 7002264

Structure parameters

• Formula: C96 H100 Cl12 Co4 N8 O5
• Calculated formula: C96 H100 Cl12 Co4 N8 O5
• Title of publication: Structural and magnetic variability of cobalt(II) complexes with bridging pyrazolate ligands bearing appended imine groups
• Authors of publication: Sachse, Anna; Demeshko, Serhiy; Meyer, Franc
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 37
• Pages of publication: 7756 - 7764
• a: 11.265 ± 0.0007 Å
• b: 15.1857 ± 0.0009 Å
• c: 17.6502 ± 0.001 Å
• α: 112.618 ± 0.004°
• β: 90.388 ± 0.005°
• γ: 106.495 ± 0.004°
• Cell volume: 2649.4 ± 0.3 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0974
• Residual factor for significantly intense reflections: 0.0688
• Weighted residual factors for significantly intense reflections: 0.1654
• Weighted residual factors for all reflections included in the refinement: 0.1775
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No