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Information card for entry 7002336
Preview
Coordinates | 7002336.cif |
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Original paper (by DOI) | HTML |
Formula | C4 H12 Cl6 O4 Ta2 |
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Calculated formula | C4 H12 Cl6 O4 Ta2 |
Title of publication | The reactivity of 1,1-dialkoxyalkanes with niobium and tantalum pentahalides. Formation of coordination compounds, C‒H and C‒C bond activation and the X-ray structure of the stable carboxonium species [Me2CCHC(OMe)Me][NbCl5(OMe)] |
Authors of publication | Marchetti, Fabio; Pampaloni, Guido; Zacchini, Stefano |
Journal of publication | Dalton Transactions |
Year of publication | 2009 |
Journal issue | 38 |
Pages of publication | 8096 - 8106 |
a | 8.17 ± 0.002 Å |
b | 9.062 ± 0.002 Å |
c | 10.634 ± 0.003 Å |
α | 75.852 ± 0.003° |
β | 89.165 ± 0.003° |
γ | 85.452 ± 0.003° |
Cell volume | 761 ± 0.3 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0581 |
Residual factor for significantly intense reflections | 0.0519 |
Weighted residual factors for significantly intense reflections | 0.164 |
Weighted residual factors for all reflections included in the refinement | 0.1674 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.191 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7002336.html
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