Information card for entry 7002598

Structure parameters

• Formula: C68 H102 N4 O8 V2
• Calculated formula: C68 H102 N4 O8 V2
• Title of publication: Synthesis, structure and ethylene polymerisation behaviour of vanadium(iv and v) complexes bearing chelating aryloxides
• Authors of publication: Homden, Damien; Redshaw, Carl; Warford, Lee; Hughes, David L.; Wright, Joseph A.; Dale, Sophie H.; Elsegood, Mark R. J.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 41
• Pages of publication: 8900 - 8910
• a: 10.5991 ± 0.0007 Å
• b: 12.9675 ± 0.0008 Å
• c: 14.7112 ± 0.0009 Å
• α: 71.2558 ± 0.001°
• β: 74.5933 ± 0.001°
• γ: 68.2679 ± 0.001°
• Cell volume: 1753.73 ± 0.19 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0463
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.0961
• Weighted residual factors for all reflections included in the refinement: 0.1038
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No