Information card for entry 7002625

Structure parameters

• Common name: (ROAl(O)DMSO)4 + 3toluene
• Formula: C101 H164 Al4 O12 S4
• Calculated formula: C101 H164 Al4 O12 S4
• Title of publication: Synthesis of aryloxyaluminium hydrides and their conversion into aryloxyalumoxanes (ArOAlO)n
• Authors of publication: Shekar, Sukesh; Taylor, Mamie M.; Twamley, Brendan; Wehmschulte, Rudolf J.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 9322
• a: 14.9642 ± 0.0005 Å
• b: 28.4632 ± 0.001 Å
• c: 50.1873 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 21376.2 ± 1.3 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0728
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.1242
• Weighted residual factors for all reflections included in the refinement: 0.1365
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No