Information card for entry 7002658

Structure parameters

• Formula: C64 H186 Cd Ge18 Si24
• Calculated formula: C64 H186 Cd Ge18 Si24
• Title of publication: [Si(SiMe3)3]6Ge18M (M = Zn, Cd, Hg): neutral metalloid cluster compounds of germanium as highly soluble building blocks for supramolecular chemistry
• Authors of publication: Henke, Florian; Schenk, Christian; Schnepf, Andreas
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 9141
• a: 14.956 ± 0.003 Å
• b: 19.083 ± 0.004 Å
• c: 23.622 ± 0.005 Å
• α: 90°
• β: 92.23 ± 0.03°
• γ: 90°
• Cell volume: 6737 ± 2 ų
• Cell temperature: 149 ± 2 K
• Ambient diffraction temperature: 149 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0783
• Weighted residual factors for all reflections included in the refinement: 0.0835
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No