Information card for entry 7002666

Structure parameters

• Formula: C42 H156 As2 N28 Ni7 O92 V8 W20
• Calculated formula: C42 H140 As2 N28 Ni7 O92 V8 W20
• Title of publication: Steric hindrance-dependent rational design and synthesis of three new Keggin-based supramolecular networks
• Authors of publication: Zhang, Xiao; Yi, Zhihui; Zhao, Liyan; Chen, Qian; Gu, Xianmo; Xu, Jiqing; Wang, Xiaolin; Yang, Chao; Xu, Xianzhu; Xia, Wujiong
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 42
• Pages of publication: 9198
• a: 19.765 ± 0.004 Å
• b: 13.618 ± 0.003 Å
• c: 27.096 ± 0.005 Å
• α: 90°
• β: 93.63 ± 0.03°
• γ: 90°
• Cell volume: 7279 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1045
• Residual factor for significantly intense reflections: 0.0769
• Weighted residual factors for significantly intense reflections: 0.2051
• Weighted residual factors for all reflections included in the refinement: 0.2232
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No