Information card for entry 7002722

Structure parameters

• Formula: H78.6 Na12.6 O86 P10 Pd15.4
• Calculated formula: Na12.555 O95 P10 Pd15.444
• Title of publication: Self-assembly of star-shaped heteropoly-15-palladate(II)
• Authors of publication: Izarova, Natalya V.; Biboum, Rosa Ngo; Keita, Bineta; Mifsud, Maria; Arends, Isabel W. C. E.; Jameson, Geoffrey B.; Kortz, Ulrich
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 43
• Pages of publication: 9385 - 9387
• a: 15.982 ± 0.005 Å
• b: 27.054 ± 0.009 Å
• c: 25.883 ± 0.008 Å
• α: 90°
• β: 103.46 ± 0.01°
• γ: 90°
• Cell volume: 10884 ± 6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.13
• Residual factor for significantly intense reflections: 0.0981
• Weighted residual factors for significantly intense reflections: 0.2264
• Weighted residual factors for all reflections included in the refinement: 0.2403
• Goodness-of-fit parameter for all reflections included in the refinement: 1.313
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No