Information card for entry 7002934

Structure parameters

• Formula: C13 H24 Cs O2 P
• Calculated formula: C13 H24 Cs O2 P
• Title of publication: A rearrangement of 1,1-linked four-membered rings to bicyclic bridgehead five-membered rings: A phosphorus turn
• Authors of publication: Ionkin, Alex S.; Marshall, William J.; Fish, Brian M.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 47
• Pages of publication: 10574 - 10580
• a: 5.9871 ± 0.0004 Å
• b: 9.5553 ± 0.0007 Å
• c: 14.2529 ± 0.001 Å
• α: 80.351 ± 0.001°
• β: 82.128 ± 0.001°
• γ: 81.032 ± 0.001°
• Cell volume: 788.87 ± 0.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0338
• Residual factor for significantly intense reflections: 0.0274
• Weighted residual factors for significantly intense reflections: 0.0635
• Weighted residual factors for all reflections included in the refinement: 0.0667
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No